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Mechanical Properties and Ion Release from Fibre-Reinforced Glass Ionomer Cement

Ivica Anja; Šalinovic Ivan; Krmek Silvana Jukic; Garoushi Sufyan; Lassila Lippo; Säilynoja Eija; Miletic Ivana

Mechanical Properties and Ion Release from Fibre-Reinforced Glass Ionomer Cement

Ivica Anja
Šalinovic Ivan
Krmek Silvana Jukic
Garoushi Sufyan
Lassila Lippo
Säilynoja Eija
Miletic Ivana
Katso/Avaa
polymers-16-00607.pdf (1.585Mb)
Lataukset: 

doi:10.3390/polym16050607
URI
https://doi.org/10.3390/polym16050607
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Julkaisun pysyvä osoite on:
https://urn.fi/URN:NBN:fi-fe2025082789254
Tiivistelmä

The aim of this study was to compare the mechanical properties and ion release from a commercially available resin-modified glass ionomer cement to a formulation reinforced by the addition of short glass fibres at various percentages. 

Methods: Three experimental groups were prepared by adding a mass ratio of 10%, 15% and 20% of short glass fibres to the powder portion of the cement from a capsule (GC Fuji II LC), while the control group contained no fibres. Microhardness (n = 12), fracture toughness, and flexural, compressive and diametral tensile strength (n = 8) were evaluated. To study ion release, readings were obtained utilising fluoro-selective and calcium-selective electrodes after 24 h, 7 days and 30 days (n = 12). The spatial distribution of fibres within the material was evaluated through scanning electron microscopy. The data were analysed using one-way ANOVA with a Bonferroni adjustment. 

Results: The findings suggest that elevating fibre weight ratios to 20 wt% results in improved mechanical properties (p < 0.05) in microhardness, flexural strength, diametral tensile strength and fracture toughness. In terms of ion release, a statistically significant difference (p < 0.001) was observed between the groups at the conclusion of 24 h and 7 days, when the fluoride release was much higher in the control group. However, after 30 days, no significant distinction among the groups was identified (p > 0.05). Regarding calcium release, no statistically significant differences were observed among the groups at any of the evaluated time points (p > 0.05). SEM showed the fibres were homogeneously incorporated into the cement in all experimental groups. 

Conclusions: Resin-modified glass ionomer enhanced with short glass fibres at a weight loading of 20% showcased the most favourable mechanical properties while concurrently maintaining the ability to release fluoride and calcium after a 30-day period.

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